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Created by Kerry Maltby
over 9 years ago
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Question | Answer |
SOCl_2 | |
i) LiAlH_4 ii) Dilute HCl (work-up) | |
Via Imines | |
Via Azides | |
1) DMSO 2) LiAlH_4 | |
1) LDA 2) LiAlH_4, Dilute HCl work-up | |
Reason for using biphasic conditions | to avoid reaction between OH- and electrophile |
Example of a biphasic solvent | NaOH |
What is a 'phase transfer' catalyst? | base that is soluble in the organic phase that is used in a biphasic reaction mixture |
Example of a 'phase transfer' catalyst | BnEt_3NCl |
1) azide, pthalimide, oxime 2) cyanide, nitromethane 3) acetonitrile |
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