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Chromatography

Bethany Westwood Chemistry AS level Englisch 15 Karten

Karten in diesem Stapel (15)

  1. 1What is the mobile phase?Carries soluble components of the mixture with it (more soluble, faster movement)
  2. 2What is stationary phase?Holds back components attracted to it (more affinity, faster)
  3. 3What apparatus is used in TLC?Glass/metal/plastic sheet coated with thin layer of silica gel or alumina (stationary phase)
  4. 4What are the advantages of TLC?- runs faster
    - small amounts can be separated
    - spots spread out less
    - plates more robust
  5. 5What happens once the solvent has run?UV light or a locating agent is used to locate the colourless spots and make them visible
  6. 6what is rf?rf = distance moved by spot/distance moved by solvent
  7. 7What is the stationary phase in column chromatography?Uses a powder (silica/aluminium oxide/resin)
  8. 8How is the apparatus set up for column chromatography?- Powder packed into narrow tube + solvent added to top
    - Eluent runs down column, components move at different rates, collected separately in flasks at bottom
    - more than 1 eluent = better separation
  9. 9What are the advantages of column chromatography?Large amounts can be separated and collected
  10. 10What is the stationary phase for gas liquid chromatography (GC)?Powder coated in oil
  11. 11What is the mobile phase for GC?unreactive gas
  12. 12What is the set up of the apparatus?- long capillary tube coiled in the oven
    - sample moves along with gas and some retained by oils (components have different retention rates)
  13. 13What is the advantage?Is very sensitive analysis
  14. 14What is GCMS?Gas chromatography mass spectrometry
  15. 15What is the process of GCMS?- GC column
    - times noted
    - into MS
    - compound indentified

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AS level Chemistry (Chapter 33 - Chromatography) Karteikarten am Chromatography, erstellt von Bethany Westwood am 10/01/2018.
Erstellt von
Bethany Westwood
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